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Change of the performance properties of nanofiltration cellulose acetate membranes by surface adsorption of polyelectrolyte multilayers

Identifieur interne : 000D16 ( PascalFrancis/Checkpoint ); précédent : 000D15; suivant : 000D17

Change of the performance properties of nanofiltration cellulose acetate membranes by surface adsorption of polyelectrolyte multilayers

Auteurs : RAMZI HADJ LAJIMI [Tunisie] ; ABDELHAMID BEN ABDALLAH [France] ; Ezdine Ferjani [Tunisie] ; MOHAMED SADOK ROUDESLI [Tunisie] ; André Deratani [France]

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Abstract

Surface modification of nanofiltration cellulose acetate (CA) membranes was carried out by alternating layer-by-layer deposition of acidic chitosan (CHI) and sodium alginate (ALG) as the cationic and anionic polyelectrolyte, respectively. The supporting CA membranes were obtained by a phase separation process from acetone/formamide (2/1 wt/wt) casting solutions using a 20 wt% polymer concentration. The pore size of the CA substrates monitored by the annealing temperature was determined from the retention values of rigid neutral solutes using the computer simulation program NanoFlux. The influence of the ultrathin multilayered polyelectrolyte surface structure on the permeability performances (water flux and ion rejection) was studied for a series of composite membranes obtained by varying the total number (up to 35) ofthe adsorbed polyelectrolyte layer pairs. SEM and permeation measurements showed that the modification mainly took place on the substrate surface so that the hydraulic permeability was only little affected by the polyelectrolyte multilayers. The permeation rate of dilute to moderate concentrated NaCl and MgSO4 solutions was found to be higher than that of pure water for some composite membranes. By comparison with the bare support, the rejection ofmonovalent salt decreased by increasing the number of adsorbed ALG/CHI layer pairs whereas that of divalent salt remained constant.


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<div type="abstract" xml:lang="en">Surface modification of nanofiltration cellulose acetate (CA) membranes was carried out by alternating layer-by-layer deposition of acidic chitosan (CHI) and sodium alginate (ALG) as the cationic and anionic polyelectrolyte, respectively. The supporting CA membranes were obtained by a phase separation process from acetone/formamide (2/1 wt/wt) casting solutions using a 20 wt% polymer concentration. The pore size of the CA substrates monitored by the annealing temperature was determined from the retention values of rigid neutral solutes using the computer simulation program NanoFlux. The influence of the ultrathin multilayered polyelectrolyte surface structure on the permeability performances (water flux and ion rejection) was studied for a series of composite membranes obtained by varying the total number (up to 35) ofthe adsorbed polyelectrolyte layer pairs. SEM and permeation measurements showed that the modification mainly took place on the substrate surface so that the hydraulic permeability was only little affected by the polyelectrolyte multilayers. The permeation rate of dilute to moderate concentrated NaCl and MgSO
<sub>4</sub>
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</fC03>
<fC03 i1="10" i2="X" l="SPA">
<s0>Dimensión poro</s0>
<s5>10</s5>
</fC03>
<fC03 i1="11" i2="X" l="FRE">
<s0>Surveillance</s0>
<s5>11</s5>
</fC03>
<fC03 i1="11" i2="X" l="ENG">
<s0>Surveillance</s0>
<s5>11</s5>
</fC03>
<fC03 i1="11" i2="X" l="SPA">
<s0>Vigilancia</s0>
<s5>11</s5>
</fC03>
<fC03 i1="12" i2="X" l="FRE">
<s0>Recuit</s0>
<s5>12</s5>
</fC03>
<fC03 i1="12" i2="X" l="ENG">
<s0>Annealing</s0>
<s5>12</s5>
</fC03>
<fC03 i1="12" i2="X" l="SPA">
<s0>Recocido</s0>
<s5>12</s5>
</fC03>
<fC03 i1="13" i2="X" l="FRE">
<s0>Rétention</s0>
<s5>13</s5>
</fC03>
<fC03 i1="13" i2="X" l="ENG">
<s0>Retention</s0>
<s5>13</s5>
</fC03>
<fC03 i1="13" i2="X" l="SPA">
<s0>Retención</s0>
<s5>13</s5>
</fC03>
<fC03 i1="14" i2="X" l="FRE">
<s0>Simulation ordinateur</s0>
<s5>14</s5>
</fC03>
<fC03 i1="14" i2="X" l="ENG">
<s0>Computer simulation</s0>
<s5>14</s5>
</fC03>
<fC03 i1="14" i2="X" l="SPA">
<s0>Simulación computadora</s0>
<s5>14</s5>
</fC03>
<fC03 i1="15" i2="X" l="FRE">
<s0>Simulation numérique</s0>
<s5>15</s5>
</fC03>
<fC03 i1="15" i2="X" l="ENG">
<s0>Numerical simulation</s0>
<s5>15</s5>
</fC03>
<fC03 i1="15" i2="X" l="SPA">
<s0>Simulación numérica</s0>
<s5>15</s5>
</fC03>
<fC03 i1="16" i2="X" l="FRE">
<s0>Structure surface</s0>
<s5>16</s5>
</fC03>
<fC03 i1="16" i2="X" l="ENG">
<s0>Surface structure</s0>
<s5>16</s5>
</fC03>
<fC03 i1="16" i2="X" l="SPA">
<s0>Estructura superficie</s0>
<s5>16</s5>
</fC03>
<fC03 i1="17" i2="X" l="FRE">
<s0>Perméabilité</s0>
<s5>17</s5>
</fC03>
<fC03 i1="17" i2="X" l="ENG">
<s0>Permeability</s0>
<s5>17</s5>
</fC03>
<fC03 i1="17" i2="X" l="SPA">
<s0>Permeabilidad</s0>
<s5>17</s5>
</fC03>
<fC03 i1="18" i2="X" l="FRE">
<s0>Rejet</s0>
<s5>18</s5>
</fC03>
<fC03 i1="18" i2="X" l="ENG">
<s0>Rejection</s0>
<s5>18</s5>
</fC03>
<fC03 i1="18" i2="X" l="SPA">
<s0>Rechazo</s0>
<s5>18</s5>
</fC03>
<fC03 i1="19" i2="X" l="FRE">
<s0>Matériau composite</s0>
<s5>19</s5>
</fC03>
<fC03 i1="19" i2="X" l="ENG">
<s0>Composite material</s0>
<s5>19</s5>
</fC03>
<fC03 i1="19" i2="X" l="SPA">
<s0>Material compuesto</s0>
<s5>19</s5>
</fC03>
<fC03 i1="20" i2="X" l="FRE">
<s0>Microscopie électronique balayage</s0>
<s5>20</s5>
</fC03>
<fC03 i1="20" i2="X" l="ENG">
<s0>Scanning electron microscopy</s0>
<s5>20</s5>
</fC03>
<fC03 i1="20" i2="X" l="SPA">
<s0>Microscopía electrónica barrido</s0>
<s5>20</s5>
</fC03>
<fC03 i1="21" i2="X" l="FRE">
<s0>Perméation</s0>
<s5>21</s5>
</fC03>
<fC03 i1="21" i2="X" l="ENG">
<s0>Permeation</s0>
<s5>21</s5>
</fC03>
<fC03 i1="21" i2="X" l="SPA">
<s0>Permeación</s0>
<s5>21</s5>
</fC03>
<fN21>
<s1>052</s1>
</fN21>
<fN44 i1="01">
<s1>OTO</s1>
</fN44>
<fN82>
<s1>OTO</s1>
</fN82>
</pA>
<pR>
<fA30 i1="01" i2="1" l="ENG">
<s1>PERMEA 2003 Membrane Science and Technology Conference of Visegrad countries</s1>
<s3>Tatranské Matliare SVK</s3>
<s4>2003-09-07</s4>
</fA30>
</pR>
</standard>
</inist>
<affiliations>
<list>
<country>
<li>France</li>
<li>Tunisie</li>
</country>
<region>
<li>Languedoc-Roussillon</li>
<li>Languedoc-Roussillon-Midi-Pyrénées</li>
</region>
<settlement>
<li>Montpellier</li>
</settlement>
</list>
<tree>
<country name="Tunisie">
<noRegion>
<name sortKey="Ramzi Hadj Lajimi" sort="Ramzi Hadj Lajimi" uniqKey="Ramzi Hadj Lajimi" last="Ramzi Hadj Lajimi">RAMZI HADJ LAJIMI</name>
</noRegion>
<name sortKey="Ferjani, Ezdine" sort="Ferjani, Ezdine" uniqKey="Ferjani E" first="Ezdine" last="Ferjani">Ezdine Ferjani</name>
<name sortKey="Mohamed Sadok Roudesli" sort="Mohamed Sadok Roudesli" uniqKey="Mohamed Sadok Roudesli" last="Mohamed Sadok Roudesli">MOHAMED SADOK ROUDESLI</name>
</country>
<country name="France">
<region name="Languedoc-Roussillon-Midi-Pyrénées">
<name sortKey="Abdelhamid Ben Abdallah" sort="Abdelhamid Ben Abdallah" uniqKey="Abdelhamid Ben Abdallah" last="Abdelhamid Ben Abdallah">ABDELHAMID BEN ABDALLAH</name>
</region>
<name sortKey="Deratani, Andre" sort="Deratani, Andre" uniqKey="Deratani A" first="André" last="Deratani">André Deratani</name>
</country>
</tree>
</affiliations>
</record>

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