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Processing and Properties of Textured Potassium Strontium Niobate (KSr2Nb5O15) Ceramic Fibers – Texture Development

Identifieur interne : 000659 ( Main/Exploration ); précédent : 000658; suivant : 000660

Processing and Properties of Textured Potassium Strontium Niobate (KSr2Nb5O15) Ceramic Fibers – Texture Development

Auteurs : Sedat Alkoy [Turquie] ; Sinan Dursun [Turquie]

Source :

Abstract

Highly [001] textured KSr2Nb5O15 (KSN) ceramic fibers were fabricated by a combination of novel alginate gelation method and templated grain growth using acicular KSr2Nb5O15 template particles. The needle‐like KSN template particles were prepared by molten salt synthesis method with salt/powder ratio of 2 giving the highest aspect ratio. Fibers were extruded into CaCl2 salt solutions from alginate‐based slurries without or with 10 wt% KSN template particles using a nozzle with 2 mm diameter and 80 mm length. Varying sintering temperature from 1300°C to 1450°C and time from 2 to 6 h were found to increase the texture. A maximum degree of orientation, ƒ(00l), of 0.95 was obtained, as measured by Lotgering factor, and a grain orientation distribution, r, of 0.28 was obtained as measured by rocking curve analysis.


Url:
DOI: 10.1111/j.1551-2916.2011.04994.x


Affiliations:


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